ESM 542 MODERN ELECTRON MICROSCOPY Spring 2000
Instructor:
Dr. Yimei Zhu, Group Leader
Electron Microscopy Facility and Nanostructure of Advanced Materials Program
Building 480
Brookhaven National Laboratory
http://www.bnl.gov/bnlweb/facilities.html
(631)-344-3057
Fax. 344-4071
zhu@bnl.gov
Class Hours:
Tuesday and Thursday
7:00 to 8:20
Physics P122.
Examinations:
Mid-Term: Thursday, March 12, 7:00 - 8:20pm
Final: To be announced.
Course Description:
Principles and practice for transmission electron microscopes. Instrument design
and operation. Electron diffraction and imaging theory. Microanalysis using x-ray,
electron spectroscopy and other advanced electron microscope techniques. Typical
EM investigations will be outlined and used as examples.
Course Outline:
The course is organized roughly in the sequence
of a typical electron microscope study:
Introduction
Basic concepts
Elastic & inelastic scattering
Instruments
Components & electron optics
Operation, alignment & calibration
Specimen preparation
Electron diffraction
Reciprocal space
Bragg reflection & diffuse scattering
Convergent-beam diffraction
Indexing spot pattern & Kikuchi pattern
Kinematical diffraction theory
Dynamic diffraction theory
Electron imaging
Diffraction contrast: two-beam method
Characterizing crystal defects (point, line & planar)
Phase contrast: HREM
Quantitative HREM & image simulation
X-ray spectroscopy
Principle & instrumentation
Quantitative x-ray microanalysis
Electron energy-loss spectroscopy
Principle & instrumentation
Quantitative microanalysis
Energy-filtering & spectroscopy imaging
Lorentz microscopy & magnetic imaging
Electron holography
Scanning transmission electron microscopy
Two TEM demonstration lectures will be included, one using Philips CM12 at
SUNY-SB, the other using JEOL3000F at BNL.
Course Requirements:
Attendence at Lectures
Timely completion of homework.
Mid-Term and Final Exams.
Background Reading.
Classroom discussion & questions are encouraged.
Grading:
Letter grades based on homework and exam scores, weighted as follows:
Homework: 25%
Mid-Term: 35%
Final: 40%
Textbook::
D.B. Williams and C.B. Carter
Transmission Electron Microscopy
Plenum (1996).
JQ.